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009371 Didechloro Vancomycin•xHCl (Vancomycin Impurity) CAS:

Specifications
References
Grade
Highly Purified
Molecular Formula
C66H77N9O24
Molecular Weight
1380.36
EU Commodity Code
38220090
Shipping Temp
Blue Ice
Storage Temp
-20°C
Vancomycin Impurity;

An impurity in Vancomycin

Melting Point
>160°C (dec.)
Solubility
Methanol (sparingly)
Method for Determining Identity
Proton NMR (D2O) and MS
TLC Conditions
C18; Methanol : Water: Ammonium Hydroxide (8 : 2 : 0.2). Visualized with UV and AMCS (Rf = 0.40).
Elemental Analysis
Found: 42.41% C; 6.09% H; 6.66% N Chloride Content: 8.7%
Storage and Stability
Store at -20°C. For maximum recovery of product, centrifuge the original vial prior to removing the cap.
Source
Synthetic
Purity
~75% with <1% Vancomycin (by HPLC)
Form
Off-white solid
References
Marshall, F.J., et al.: J. Med. Chem., 8, 18 (1965), Sheldrick, G.M., et al.: Nature, 271, 223 (1987), Dutca-Melan, S., et al.: J. Clin. Microbiol., 33, 24 (1995),
USBio References
No references available
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