421595
CAS Number
145119-17-1Grade
Highly PurifiedMolecular Formula
C₁₁H₁₉NO₄Molecular Weight
229.27EU Commodity Code
38220090Shipping Temp
RTStorage Temp
-20°C(2E)-6-[[(1,1-Dimethylethoxy)carbonyl]amino]-2-hexenoic Acid
(E)-6-[[(1,1-Dimethylethoxy)carbonyl]amino]-2-hexenoic Acid
(2E)-6-[[(1,1-Dimethylethoxy)carbonyl]amino]-2-hexenoic Acid is an intermediate in the synthesis of (E)-6-Amino-2-hexenoic Acid, used in the preparation of anti-collagenase active agent.
Synonym
(E)-6-[[(1,1-Dimethylethoxy)carbonyl]amino]-2-hexenoic Acid
Molecular Formula
C₁₁H₁₉NO₄
Appearance
White to off-white solid
Melting Point
55-59ºC (lit)
Solubility
Chloroform (Slightly), Methanol (Slightly)
Method for Deterining Identity
Proton NMR Spectroscopic and Mass Spectrometric Analysis
TLC Conditions
SiO2; Ethyl Acetate: Hexanes=7;3; Visualized with UV and KMnO4; Single Spot, Rf=0.65
Elemental Analysis
Calculated: %C: 57.62, %H: 8.35, %N: 6.11
Storage and Stability
Store at -20°C. Caution: Hygroscopic; Store under inert atmosphere. For maximum recovery of product, centrifuge the original vial prior to removing the cap.
Intended for research use only. Not for use in human, therapeutic, or diagnostic applications.
References
1. Banfi, L., et al.: J. Org. Chem., 73, 1608 (2008). 2. Yoshitomi, Y., et al.: Tetrahedron., 64, 11568 (2008)USBio References
No references available